Distillation Glassware

Photo of Corning 3360 PYREX® General Purpose Distilling Apparatus with Standard Taper Stopper and 19/38 Standard Taper Joint

These PYREX® general purpose batch distillation apparatus allow the addition of reagents via the No. 27 Standard Taper PYREX® stoppered neck. It is ideally suited for the batch production of high purity distilled water. The flask has a flat bottom with a side delivery tube, terminating in a 19/38 Standard Taper joint. Graham condenser tubulations are 10mm O.D. For replacement stoppers, see No. 7650. For replacement condensers, see No. 2540-200.

Photo of PYREX® Water By Distillation Receiver

For determining water by distillation. Receivers have a 24/40 Standard Taper ground joint on the sidearm.The 10mL receiver is graduated from 0 to 1mL in 0.1mL intervals with a maximum scale error of 0.05mL. Graduation intervals from 1.0 to 10.0mL are 0.2mL with maximum scale error of 0.1mL.The 25mL receiver is graduated from 0 to 1mL in 0.1mL intervals with a maximum scale error of 0.05mL. Graduation intervals from 1.0 to 25.0mL are 0.2mL with a maximum scale error of 0.1mL. Inner and outer joint sizes are 24/40 Standard Taper ground joint.

Photo of Cyanide Distillation Kit. Wheaton
Cyanide distillation kit with Clear-Seal® Joints This unit is manufactured from Wheaton 33® low extractable borosilicate glass (meets ASTM Type I Class A and USP Type I standards). Use this kit for removing interfering substances in quantitative analysis for cyanide. The sample is reacted with H2SO and MgCl2, which converts any cyanide to HCN. HCN distills over and is absorbed in a NaOH solution, which is then analyzed for CN. Reference: ASTM D-2036-87.
Photo of Kimble KIMAX 21500 Distilling Apparatus with Full Length 19/38 Joints

Kimble KIMAX 21500 Distilling Apparatus with Full Length 19/38 Joints is used for general purpose distillation and phenol distillation. Flask has a flat bottom and a distillation head with a full length 19/38 joint. Supplied with a  stopper. Condenser is Graham-style having a 200 mm jacket with a full length 19/38 joint at the top only. For method, reference APHA Examination of Water and Wastewater: Method 4500-NH3 nitrogen (ammonia) in purified drinking water, natural water, and highly purified wastewaters (concentration < 20 μg/L).

Photo of Corning 3602-10 PYREX 10mL Dean Stark Distilling Receiver

This 10mL PYREX® Dean Stark distilling receiver is graduated from 0 to 1mL in 0.1mL intervals, with a maximum scale error of 0.05mL. The graduation intervals from 1.0 to 10.0mL are 0.2mL, with a maximum scale error of 0.1mL. Reference: ASTM E-123.

(Sample Photo Displayed. Individual items may differ from the image shown.)

 

Photo of PYREX® Oil Dilution Distilling Receiver
For determining the amount of dilution in crankcase oils when gasoline has been used as fuel. Designed to allow heat-sensitive materials to be kept away from the hot base of the flask. With an outer 24/40 joint at the top and an inner 24/40 joint on the sidearm.
Photo of Corning 3622-20 PYREX Barrett Distilling Apparatus

PYREX® Barrett Distilling Apparatus with Stopcock and 24/40 Standard Taper Joints This PYREX® distilling apparatus is for determining water content in petroleum or bituminous products. It is graduated upwards from the stopcock to 3mL in 0.2mL divisions, and from 3mL to 20mL in 0.5mL divisions. For replacement stopcock plugs, see No. 7680. For replacement retaining clips, see No. 7280. Reference: Barrett method B-2.

Photo of KIMBLE® 21802 KIMAX® Vigreux Distillation Column with 19/22 Joints and Drip Tip

KIMBLE® 21802 KIMAX® Vigreux Distillation Column with Drip Tip. The 200mm long column has a 19/22 outer joint at the upper end and a 19/22 inner joint at the lower end. Drip tip is provided at the lower end. Inner tube has twelve sets of rings of indentations spaced approximately 14 mm apart. Sets are alternately horizontal and slanted downward.  Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements.

(Sample Photo Displayed. Individual items may differ from the image shown)

 

Photo of KIMBLE® 22012 KIMAX® Modified Dean-Stark Distilling Receiver with Full Length 24/40 Joints

KIMBLE® 22012 KIMAX® Modified Dean-Stark Distilling Receiver with Full Length 24/40 Joints and a siphon return arm.  Sidearm bridge equalizes pressure. Designed from ASTM Specification E123, Style A. 

(Sample Photo Displayed. Individual items may differ from the image shown)

 

Photo of KIMBLE® 21805 KIMAX® Jacketed 300mm Distillation Column with Full Length 24/40 Joints

KIMBLE® 21805 KIMAX® Jacketed 300mm Distillation Column with Full Length 24/40 Joints. This column is a one-piece sealed unit with a 24/40 outer joint at the upper end and a 24/40 inner joint at the lower end. Drip tip is provided at the lower end. Inner tube has a single ring of indentations near the exit end to support packing material. Supplied with a jacket so the column may also be used as a condenser. Hose connections accept 5/16" I.D. flexible tubing. Inner tube I.D. is 13.5mm.

(Sample Photo Displayed. Individual items may differ from the image shown)